TY - JOUR
T1 - Calibration of the B54X channel and implementation of k0-NAA at the RA3-reactor, Ezeiza, Argentina
AU - Jasan, R.C.
AU - Invernizzi, R.
AU - Vermaercke, Peter
A2 - Sneyers, Liesel
N1 - Score = 10
PY - 2014/3/4
Y1 - 2014/3/4
N2 - The B54X position of the 8 MW RA3 research
reactor at the Ezeiza Atomic Centre of the Argentine
National Atomic Energy Commission is currently being
used for NAA irradiations. The facility with a nominal
average fluence of 5 9 1013 cm-2 s-1 is dedicated to long
irradiations of up to 5 h. Samples are being measured after
a decay of typically 7 and 30 days. With the aim of
implementing the k0-NAA method at the Nuclear Analytical
Techniques Laboratory of the Centre, the reactor
parameters a and f were estimated applying multi monitor
methods using the Kayzero for Windows software. After a
careful recalibration of the HPGe detector, SMELS III,
NIST SRM 1633b and several other matrix RM’s were
analyzed using the k0 standardization in order to verify the
proper implementation of the k0-NAA approach. The found
accuracy and associated uncertainties are discussed. In
general, good agreement was obtained between results of
this work and the reference values of the individual reference
materials, thus proving successful first implementation
of the above method and trueness of the results
achieved. The obtained detection limits for several elements
were evaluated.
AB - The B54X position of the 8 MW RA3 research
reactor at the Ezeiza Atomic Centre of the Argentine
National Atomic Energy Commission is currently being
used for NAA irradiations. The facility with a nominal
average fluence of 5 9 1013 cm-2 s-1 is dedicated to long
irradiations of up to 5 h. Samples are being measured after
a decay of typically 7 and 30 days. With the aim of
implementing the k0-NAA method at the Nuclear Analytical
Techniques Laboratory of the Centre, the reactor
parameters a and f were estimated applying multi monitor
methods using the Kayzero for Windows software. After a
careful recalibration of the HPGe detector, SMELS III,
NIST SRM 1633b and several other matrix RM’s were
analyzed using the k0 standardization in order to verify the
proper implementation of the k0-NAA approach. The found
accuracy and associated uncertainties are discussed. In
general, good agreement was obtained between results of
this work and the reference values of the individual reference
materials, thus proving successful first implementation
of the above method and trueness of the results
achieved. The obtained detection limits for several elements
were evaluated.
KW - Neutron activation analysis
KW - k0-NAA
KW - Reactor calibration
KW - Detector calibration
UR - http://ecm.sckcen.be/OTCS/llisapi.dll/open/ezp_136818
UR - http://knowledgecentre.sckcen.be/so2/bibref/11790
U2 - 10.1007/s10967-014-3067-4
DO - 10.1007/s10967-014-3067-4
M3 - Article
SN - 0236-5731
VL - 300
SP - 489
EP - 497
JO - Journal of Radioanalytical and Nuclear Chemistry
JF - Journal of Radioanalytical and Nuclear Chemistry
IS - 2
ER -